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Wellington Reporters 2013 - 2022 | Wellington Laboratories | Greyhound Chromatography

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NEW CATALOGUE ANNOUNCEMENT 23 DECEMBER, 2021

Wellington Laboratories Catalogue Announcement

PERFLUORINATED COMPOUNDS, OCTOBER 2021

Native & Mass-Labelled PFAS Mixtures Compatible with U.S. EPA Draft Method 1633

Native and Mass Labelled PFAS Standards Image

Wellington Laboratories is pleased to support U.S. EPA draft Method 1633 for the analysis of PFAS in aqueous, solid, biosolid, and tissue samples by releasing compatible prime stock solutions.  To offer the greatest degree of flexibility with other applications, a series of native (PFAC-MXF, PFAC-MXG, PFAC-MXH, PFAC-MXI and PFAC-MXJ) and mass-labelled (MPFAC-HIF-ES and MPFAC-HIF-IS) stock solutions have been prepared.  These mixtures can be diluted and/or combined to achieve the spiking a calibration solutions recommended by the method. 

 

PERFLUORINATED COMPOUNDS, NOVEMBER 2020

Native PFAS Certified Reference Standards
L-PFUdS      L-PFTrDS    EU-5813-NSS


In November the European Parliament and the Council of the European Union released new requirements for the analysis of per- and polyfluoroalkyl substances (PFAS) in water intended for human consumption (5813/20). Unfortunately, this amendment to Council Directive 98/83/EC included perfluoroalkanesulfonates that were not commercially available.  In response to this Wellington Laboratories synthesized, purified, characterized and prepared accurate certified reference standards of the required substances: sodium perfluoro-1-undecanesulfonate (L-PFUds) and sodium perfluoro-1-tridecanesulfonate (L-PFTrDS).  We have also prepared a native solution/mixture (EU-5813-NSS) that contains all of the PFAS listed in the drinking water directive (5813/20) for your convenience,  This solution/mixture can be used in conjunction with two of Wellington's existing mass-labelled PFAS mixtures to easily prepare a calibration set for quantification. 

PFAS Structures Image

PERFLUORINATED COMPOUNDS, NOVEMBER 2020

ISO 21675:2019 Solution/Mixtures
ISO 21675-NSS     ISO-21675-LSS

To supoport the international standard for water quality (ISO 21675:2019) which can be utilized to determine perfluoroalkyl and polyfluoroalkyl substances (PFAS) in various water samples using solid phase extraction and LC-MS/MS analysis, Wellington Laboratories has prepared native and mass-labelled solution/mixtures (Iso 21675-NSS & ISO 21675-LSS respectively.  These solutions will allow analytical laboratories to reduce the time and cost associated with solution prpraration with solution preparation and testing by purchasing ready made certified standrdas.  This flexible method allows for the analysis of a variety of waters including fresh water, sea water, and waste water containing less than 2 g/L solid particulate material for a selection of PFAS with varying functionality.

Chromatogram Image ISO-21675-NSS

PERFLUORINATED COMPOUNDS, JANUARY 2020

Native PFAS Solution/Mixtures
PFAC-MXF   PFAC-MXG

The removal of PFOS and PFOA from industrial processes has resulted in increased use of replacement per- and polyfluoroalkyl substances (PFAS) such as Gen x (HFPO-DA), ADONA (NaDONA), and F-53B (9Cl-PF3ONS and 11Cl-PF3OUdS).  Wellington Laboratories previously released individual Certified Reference Standards for these compounds, and has now generated a solution/mixture that can be used to reduce the cost of in-house solution preparation as laboratory methods are modified to incorporate these new analytes in accordance with U.S. EPA Method 537 (revision 1.)

Similarly, the finalisation of U.S. EPA Method 533 has prompted many commercial laboratories to expand their PFAS analyte list to include the replacement PFAS listed above as well as three new perfluoroether- and perfluoropolyether-carboxylic acids (PF4OPeA, PF50HxA and 3,6-OPFHpA) and a perfluoropolyethersulfonate (PFEESA).  To accommodate laboratories doing drinking water analyses, Wellington Laboratories has also added a new solution/mixture of native perfluoroethercarboxylic acids and a perfluoroethersulfonate (PFAC-MXG) to their PFAS product line.  Although Wellington Laboratories offers both native (EPA-533PAR) and mass-labelled (EPA-533ES & EPA5331S) certified primary dilution standards for EPA Method 533, PFAC-MXG can be conbined with PFAC-MXF and PFAC-24PAR to easily generate a qulaity control standard (QCS) for this method as well. 

 

 

PERFLUORINATED COMPOUNDS

Aqueous Film-Forming Foam PFAS
5:3FTB   5:1:2FTB


Interest in novel zwitterionic and cationic per- and polyfluoroalkyl substances (PFAS) being found at sites exposed to aqueous film-forming foams (AFFFs) continues to arise.  As such, Wellington Laboratories has expanded their PFAS product line to include two additional zwitterionic AFFF compounds (5:3FTB and %:1:2FTB).  It has been reported in scientific literature that environmental concentrations of fluorotelomer betaines (FTBs) do not decrease as quickly as fluorotelomer sulfonamide alkylbetaines (FTABs).  This makes research associated with the mobility of these compounds as well as their environmental monitoring very important. 

Aqueous film-foaming Foam PFAs Structure Image

HALOGENATED FLAME RETARDANTS & RELATED COMPOUNDS, DECEMBER 2019

Native Organophosphate Reference Standards
3tBPDPP   T3tBPP   B3tBPPP   T24DtBPP    3IPPDPP   B3IPPPP   

In order to aid researchers in the accurate quantitation of organophosphorous compounds in environemntal samples, Wellington laboratories has produced certified reference standards for 6 new native organophosphate compounds that are believed to be present at significant levels in commercial flame retardant mixtures.  These new products complement Wellington's existing inventory of native and mass-labelled organophosphate reference standards. 

Native Organophosphate Reference Standards Structures

 

 

HALOGENATED FLAME RETARDANTS & RELATED COMPOUNDS

Dechlorinated anti-Dechlorane Plus®
axCl11DP   axxCl10DP
Dechlorane Plus (DP), an additive polychlorinated flame retardant with a variety of applications, has been detected as an environmental contaminant on a global scale.  Due to rising concerns regarding the presence of DP and its related compounds in environmental samples, Wellington Laboratories has expanded their DP products line to include additional certified reference standards for dechlorinated anti-DP (axCl1 1DP and axxCl10DP.

Dechlorinated anti-dechlorane Plus Structures Image

 

PERFLUORINATED COMPOUNDS, NOVEMBER 2019

New PFAS Reference Standard Solutions
PF4OPeA (PFMPA)   PF5OHxA (PFMBA)   3,6-OPFHpA (NFDHA)   
P5MeODIOXOAc (C6O4)   PFEESA   FDSA-I   N-MeFBSA-M

In response to customer requests Wellington Laboratories expanded their PFAS product line to include four new perfluoroether- and perfluoropolyether-carboxylic acids (PF40PeA, PF50HxA, 3,6-OPFHpA and P5MeODIOXOAc), a perfluoroethersuphonate (PEESA), perfluorodecanesulfonamide (FDSA-1), and N-methylperfluorobutanesulfonamide (N-MeFBSA-M). 

Perfluoroalkyl Substances Structures, Image

PERFLUORINATED COMPUNDS, NOVEMBER 2019

New PFAS Solution/Mixture
PFAC30PAR

Wellington Laboratories has prepared a native/solution mixture which expands on the analyte list of their popular PFAC-24PAR product.  The updated mixture contains 6 additional analytes including HFPO-DA, NaDONA, 9Cl-PF3ONS, 11Cl-PF3OUdS, FBSA, and FHxSA.  In addition, the N-MeFOSAA and N-EtFOSSA components of PFAC30PAR are charachterized mixtures in the branched and linear and branched isomers C6 and C8 perfluoroalkanesulfonates (PFHxSK and PFOSK).

The mass-labelled solution/mixture MPFAC-24ES can still be used in combination with M3HFPO-DA to create a mixture containing suitable surrogates for the PFAC30PAR.

PFAC30PAR Chromatogram Image

CERTIFIED REFERENCE MATERIALS, JANUARY 2019

Reference Fish Tissue & Extract
WMF-02   WMF-03   WMF-EX
In response to customer requests for an expanded selection of certified environmental reference materials (ERMs) Wellington Laboratories conducted an inter laboratory study in 2018 and was able to characterize three seperate fish materials for select persistent organic pollutants.  Certified analyte concentrations were derived using data received from at least 10 analytical laboratories accredited to ISO/IEC 17025 and data were statistically analyzed using the Q-method/Hampel estimator (robust method, ISO 13528:2015).  As a result Wellington Laboratories added WMF-02, WMF-03 and WMF-EX to their product line of  Environmental Reference Materials. 

 

PERFLUORINATED COMPOUNDS, AUGUST 2018

Aqueous Film-Forming Foam PFAS
FBSA-I   FHxSA-I  N-AP-FHxSA
N-TAmP-FHxSA   N-CMAmP-6:2FOSA (6:2FTAB)

In response to ever increasing reports of novel zwitterionic and cationic PFAS contaminants being found at sites exposed to aqueous film-forming foams (AFFFs), Wellington Laboratories has expanded their PFAS product line to include three zwitterionic AFFF compounds, N-AP-FHxSA and N-CMAmP-6:2FOSA (which is commonly referred to as 6:2FTAB in the scientific literature), as well as neutral compounds also detected at impacted sites (FHxSA-1 and FBSA-1).

Aqueous Film Foaming Foam PFAS Structure

HALOGENATED FLAME RETARDANTS AND RELATED COMPOUNDS, AUGUST 2018

Mass-Labelled anti-Dechlorane Plus®
Ma-DP

Dechlorane Plus (DP) is a current use additive polychlorinated flame retardant with a variety of applications including electronic cables and wiring and plastic building materials.  Due to a rising concerns regarding the presence of DP and its related compounds, in environmental samples, Wellington Laboratoreies has expanded their product line to include a mass-labelled anti-DP certified reference standard which it is hoped will aid the analysis of this group of compounds. 

Mass-labelled anti-Dechlorane Plus Structure Image

ADDITIONAL PRODUCTS, AUGUST 2018

Polychlorinated Naphthalenes
PCN Window Defining Solution/Mixture (PCN-WD)
PCN Major Halowax Congeners Solution/Mixture (PCN-HWX)
PCN Major Incineration Congeners Solution/Mixture (PCN-INC)
PCN Potentially Toxic Congeners Solution/Mixture (PCN-TOX)

Although the industrial production of polychlorinated naphthalenes (PCNs) ceased in the 1970/1980s, their persistence in the environment as well as their formation during incineration processes has resulted in an ongoing demand for certified reference standards for this group of compounds.  In resonse to customer requests, Wellington Laboratories has expanded their line of native PCNs and prepared mixtures that we hope will aid laboratories in their analysis of these persistent organic pollutants (POPs).

Wellington Laboratories have made available a PCN window defining solution/mixture (PCN-WD), two PCN major congeners solutions/mixtures (PCN-HWX and PCN-INC), and a PCN potentially toxic congeners solution/mixture (PCN-TOX). 

Polychlorinated Naphthalenes Structure Image

ADDITIONAL PRODUCTS, AUGUST 2018

Native and Mass-Labelled Organochlorine Pesticides
Native OC Pesticide Solution/Mixture (OCP-MXA)
Mass-Labelled OC Pesticide Solution/Mixture (MOCP-MXA)
Native DDT & Related Compound Solution/Mixture (DET-MXA)
Mass-Labelled DDT & Related Compound Solution/Mixture (MDET-MXA)
Native HCH Solution/Mixture (HCH-MXA)
Mass-Labelled HCH Solution/Mixture (MHCH-MXA)

 

 

FLUORINATED COMPOUNDS, APRIL 2018

Native Reference Standards for U.S. EPA Method 537
br-NMeFOSAA   br-NEtFOSAA  EPA-537PDS  EPA-537PDS-L

PERFLUORINATED COMPOUNDS, AUGUST 2017

Native Reference Standard for Perfluoro-4-ethylcyclohexanesulfonate
PFECHS

MASS-LABELLED CHLORINATED DIBENZO-P-DIOXINS

Mass-Labelled Dichloro[13C12]dibenzo-p-dioxins
MDD-27    MDD-28

HALOGENATED FLAME RETARDANTS & RELATED COMPOUNDS

Native HBCD Enantiomer Reference Standards
(+)aHBCD   (-)aHBCD   (+)gHBCD   (-)gHBCD

PERLUORINATED COMPUNDS, NOVEMBER 2016

PFAC-24PAR (contains brPFHxS and brPFOS)
MPFAC-24ES

HALOGENATED FLAME RETARDANTS & RELATED COMPOUNDS

Native Organophosphate Reference Standards
B2tBPPP   B4tBPPP   2tBPDPP   4tBPDPP   T4tBPP
T3IPPP   T4IPPP   T34DMPP  B24DIPPPP  B2IPPPP
B4IPPPP   2IPPDPP  4IPPDPP   24DIPPDPP
PERFLUORINATED COMPOUNDS, AUGUST 2016

Reference Standards for ADONA and F-53B
NaDONA
9Cl-PF3ONS
11Cl-PF3OUdS

PERFLUORINATED COMPOUNDS, AUGUST 2016

Sodium perfluoro-1-propanesulfonate: L-PFPrS

BROMINATED FLAME RETARDANTS & RELATED COMPOUNDS, OCTOBER 2015

Native Tris(2,3-dibromopropyl) phosphate: TDBPP

 

PERFLUORINATED COMPOUNDS, SEPTEMBER 2015

Mass-Labelled Perfluorobutanesulfonate
M3PFBS

PERFLUORINATED COMPOUNDS, JUNE 2015

Native Telomer Sulfonate
10:2FTS

PERFLUORINATED COMPOUNDS, JUNE 2015

Native Branched Perfluorinated Compounds
NaP3MHpS   P3MHpA   P4MOA

PERFLUORINATED COMPOUNDS, APRIL 2015

Native Perfluorinated Compounds
NaP6MHpS   P355TMHxA   5:2sFTOH

ADDITIONAL PRODUCTS, APRIL 2015

Native Halogenated Carbazole
BCZ-36

PERFLUORINATED COMPOUNS, SEPTEMBER 2014

Native Telomer Acrylates, Telomer Acetates, Chloro-PFOS, and a branched PFCA
8:2FTAcr   10:2FTAcr   8:2FTOAc  10:2FTOAc
8Cl-PFOS   P37DMOA

ADDITIONAL PRODUCTS, SEPTEMBER 2014

Native and Mass-Labelled Halogenated Carbazoles
CCZ-3   CCZ-36    CCZ-1368   CCZ-2367   BCZ-3   BCZ-27
BCZ-136   BCZ-1368   1-B-36-CCZ   18-B-36-CCZ  MCCZ-36   MCCZ-1368

ADDITIONAL PRODUCTS, JUNE 2014

Native and Mass-labelled Tetrachlorodibenzothiophenes
TCDT-83   TCDT-85   MTCDT-85

PERFLUORINATED COMPOUNS, APRIL 2014

Mass-Labelled Telomer Sulfonates
M2-4:2FTS   M2-8:2FTS

BROMINATED FLAME RETARDNATS & RELATED COMPOUNDS, MAY 2014

Native and Mass-labelled Reference Standards
TBBA   MTBBA   MeTBBA   TBPAn   MTBPAn

PERFLUORINATED COMPOUNDS, APRIL 2014

Native 8-Chloroperfluorooctylphosphonic Acid
Cl-PFOPA

PERFLUORINATED COMPOUNDS, MARCH 2014

Native Polyfluorinated Phosphate Ester
6:2/8:2diPAP

PERFLUORUINATED COMPOUNDS, MARCH 2014

Native Polyfluorinated Phosphate Esters (SAmPAPs)
SAmPAP   diSAmPAP

BROMINATED FLAME RETARDNATS & RELATED COMPOUNDS, AUGUST 2013

Mass-Labelled Reference Standards
MEHTBB   MBEHTBP

ADDITIONAL PRODUCTS, AUGUST 2013

Native and Mass-Labelled Bisphenol A & Native Bisphenol Analogues
BPA   MBPA   BPAF   BPAP   BPB   BPF  BPP   BPS   BPZ

BROMINATED FLAME RETARDANTS & RELATED COMPOUNDS, MAY 2013

TEP & dTEP   TPrP & dTPrP   TBP & dTBP   TBEP & M6TBEP   EHDP
TEHP   TCEP & dTCEP   TCPP   TDCPP & dTCDPP   dBDCP   dTPP

BROMINATED FLAME RETARDANTS & RELATED COMPOUNDS,MARCH 2013

Halogenated Flame Retardant
Dec-604CB

BROMINATED FLAME RETARDANTS & RELATED COMPOUNDS,MARCH 2013

Native and Mass-Labelled HBCD Solution/Mixtures
HBCD-MXA   MHBCD-MXA

PERFLUORINATED COMPOUNDS, FEBRUARY 2013

Native and Mass-labelled Hexafluoropropylene Oxide Dimer Acid
(technical product known as GenX)
HFPO-DA   M3HFPO-DA

BROMINATED FLAME RETARDANTS & RELATED COMPOUNDS, DECEMBER 2012

Halogenated Flame Retardants
1,3-DPMA   DBCD   Dec-601   Dec-602   Dec-603   Dec-604
CPlus   DBALD   HCPN

PERFLUORINATED COMPOUNDS, DECEMBER 2012

Mass-Labelled Perfluoroalkylcarboxylic Acids
M2PFTeDA   M2PFHxDA

l Range of Wellington Laboratories' Products

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