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GC DERIVATISATION REAGENTS

             

A large number of reagents are used to prepare derivatives for gas chromatography, but most of the derivatization reactions fit into one of three categories: acylation, alkylation, or silylation. This bulletin describes each category, and presents information on how to choose the proper reagent based on the functional group(s) of the compound to be derivatized.

 

An extensive range of Derivitisation Reagents are available from Sigma Aldrich and Macherey-Nagel.   If you do not see the reagent you are looking for please email sales@greyhoundchrom.com  We will be happy to source it for you.

Sigma Aldrich Guide to Derivatization Reagents for GC

 

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TMSH (0.2 M in Methanol)

Part Number: 701520.101
Pack Size: 10x1mL
£168.30
Trimethylsulphonium hydroxide (0.2 M in Methanol)

MBHFBA

Part Number: 701420.201
Pack Size: 20x1mL
£580.96
N-methyl-bis(heptafluorobutyramide)

BSA

Part Number: 701210.510
Pack Size: 5x10mL
£153.72
N,O-bis-trimethylsilyl-acetamide

MSTFA

Part Number: 701270.1100
Pack Size: 1x100mL
£627.07
N-methyl-N-trimethylsilyl-trifluoroacetamide

Derivatisation Method Development Kit

Part Number: 701952
Pack Size: Kit
£135.25
Derivatisation Kit (2 x 1mL each of TMSH, MSTFA and MBTFA)

HMDS

Part Number: 52619-250ML
Pack Size: 1x250mL
£150.00
Hexamethyldisilazane